HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzylic alcohol → 1,4-Difluoro-2-(3-fluoro-benzyloxy)-5-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzylic alcohol | HCID 68008 | — |
| Reactant | 1,2,4-Trifluoro-5-nitrobenzene | HCID 75012 | — |
| Product | 1,4-Difluoro-2-(3-fluoro-benzyloxy)-5-nitrobenzene | HCID 21920037 | 55% |
Reaction Steps
Prepared in analogy to example 1a) from 2,4,5-trifluoronitrobenzene and 3-fluoro-benzyl alcohol. Colorless solid. Yield=55%. MS: m/e=283.1 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762320B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-826d26576fa443b5b2b5be48f43ecbd7 |
| Source note | uspto-grants-2004_07 |