HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzaldehyde → 4-[2-(4-Chloro-phenyl)-vinyl]-1-nitro-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Reactant | Diethyl 4-nitrobenzylphosphonate | HCID 256065 | — |
| Product | 4-[2-(4-Chloro-phenyl)-vinyl]-1-nitro-benzene | HCID 155415 | 95% |
Reaction Steps
Prepared in analogy to example 56b) from (4-nitro-benzyl)-phosphonic acid diethyl ester and 4-chloro-benzaldehyde. Yellow solid. Yield=95%. MS: m/e=259.1 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762320B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-9474082fc1d5402cade11d2754f5d944 |
| Source note | uspto-grants-2004_07 |