HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(1-Aminonaphthalen-4-yloxy)-2h-pyran-2-one hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | [4-(2-oxo-2H-pyran-4-yloxy)-naphthalen-1-yl]-carbamic acid tert-butyl ester | HCID 11439599 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4-(1-Aminonaphthalen-4-yloxy)-2h-pyran-2-one hydrochloride | HCID 23505806 | — |
Reaction Steps
A mixture of [4-(2-oxo-2H-pyran-4-yloxy)-naphthalen-1-yl]-carbamic acid tert-butyl ester (0.287 g) and HCl (2 mL of a 4N solution in dioxane) in 4 mL of dioxane was stirred overnight, diluted with ether and filtered. The filtrate was dried providing 4-(4-amino-naphthalen-1-yloxy)-pyran-2-one hydrochloride salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06765009B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-ae4974a70fd049d8ad985f4467709788 |
| Source note | uspto-grants-2004_07 |