HRID1884613

反应详情

EQUATION

反应方程式

HRID 1884613 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of [4-(2-oxo-2H-pyran-4-yloxy)-naphthalen-1-yl]-carbamic acid tert-butyl ester (0.287 g) and HCl (2 mL of a 4N solution in dioxane) in 4 mL of dioxane was stirred overnight, diluted with ether and filtered. The filtrate was dried providing 4-(4-amino-naphthalen-1-yloxy)-pyran-2-one hydrochloride salt.

WORKUP

后处理

  1. filtrationfiltered
  2. customThe filtrate was dried