Sulfuric Acid → HCID 131717505, compound

Participants

Reaction Conditions

Reaction Steps

The procedure is as in Example B, but 9.9 g of 98% 2-ethylhexylamine are introduced in the course of 20 minutes into an aqueous solution containing 15.44 g of sodium molybdate and kept at 60° C. After heating at 60° C. for 45 minutes, the mixture is acidified with 23.1 g of 30% sulphuric acid, before washing and drying the product. The latter is in the form of a white solid containing 36.8% of molybdenum and 4.38% of nitrogen.

Provenance & Evidence