Sulfuric Acid → HCID 131717505, compound

HRID 1885098Notes

Reaction equation

HRID 1885098 reaction equation
[CH2:1]([CH:3]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:4][NH2:5])[CH3:2].[O-][Mo:11]([O-])(=O)=O.[Na+].[Na+].S(=O)(=O)(O)O>>[CH2:1]([CH:3]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:4][NH2:5])[CH3:2].[Mo:11]

Participants

4

Reactant 3

HCID 1118Sulfuric AcidHCID 77192-EthylhexylamineHCID 61424Sodium Molybdate

Product 1

HCID 131717505HCID 131717505, compound

Conditions

Temperature
60 °C

Procedure

The procedure is as in Example B, but 9.9 g of 98% 2-ethylhexylamine are introduced in the course of 20 minutes into an aqueous solution containing 15.44 g of sodium molybdate and kept at 60° C. After heating at 60° C. for 45 minutes, the mixture is acidified with 23.1 g of 30% sulphuric acid, before washing and drying the product. The latter is in the form of a white solid containing 36.8% of molybdenum and 4.38% of nitrogen.

Workup

  1. additionare introduced in the course of 20 minutes into an aqueous solution
  2. customkept at 60° C
  3. washbefore washing
  4. customdrying the product
  5. additioncontaining 36.8% of molybdenum and 4.38% of nitrogen

Sources & evidence

ORD record
ord-8df74b87d2474044893af0baf3e32f83
Source dataset
uspto-grants-1992_09
Patent number
US05143633

Reaction notes

Loading…