Sulfuric Acid → HCID 131717506, compound

HRID 1885099Notes

Reaction equation

HRID 1885099 reaction equation
[O-][Mo:2]([O-])(=O)=O.[Na+].[Na+].S(=O)(=O)(O)O.[CH2:13]([C:25]1[CH:31]=[CH:30][C:28]([NH2:29])=[CH:27][CH:26]=1)[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>>[CH2:13]([C:25]1[CH:26]=[CH:27][C:28]([NH2:29])=[CH:30][CH:31]=1)[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24].[Mo:2]

Participants

4

Reactant 3

HCID 1118Sulfuric AcidHCID 77014-DodecylanilineHCID 61424Sodium Molybdate

Product 1

HCID 131717506HCID 131717506, compound

Procedure

The procedure is as in Example A, but an aqueous solution containing 48.4 g of sodium molybdate is acidified with 65.4 g of 30% sulphuric acid. While the solution is kept at 60° C., 52.2 g of p-dodecylaniline are added.

Workup

  1. customis kept at 60° C.

Sources & evidence

ORD record
ord-8f0c29be71a44b9f933e9ae9ec4c8890
Source dataset
uspto-grants-1992_09
Patent number
US05143633

Reaction notes

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