1-Iodopropane → HCID 22112627, compound

Participants

Reaction Steps

160 g of methyl D-lactate and 524 g of 1-iodopropane were mixed in a four-necked flask, and 471 g of freshly prepared Ag2O was gradually added. Then, the mixture was stirred at 60°-65° C. for 1 hour and subjected to filtration. The filtrated product was washed with ether and the ether was distilled off from the filtrate, which was then distilled in vacuo to obtain 161 g of methyl 2-propoxypropionate.

Provenance & Evidence