HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopentane → HCID 14693034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopentane | HCID 12335 | — |
| Reactant | (L)-ethyl lactate | HCID 92831 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14693034 | HCID 14693034 | 43.5% |
Reaction Steps
98 g of ethyl L-lactate, 313 g of 1-iodopentane and 245 g of freshly prepared Ag2O were stirred at 60°-65° C. for 16 hours, and diluted with ether, followed by removal of insoluble matter by filtration. After distilling off the ether, the reaction liquid was distilled in vacuo to obtain 68 g of ethyl 2-pentyloxypropionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05143643 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-a421a0b008d14cd7935990647272d82c |
| Source note | uspto-grants-1992_09 |