4-Toluenesulfonyl chloride → HCID 19808482, compound

HRID 1885152Notes

Reaction equation

HRID 1885152 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[N:13]2[CH2:18][CH2:17][N:16]([CH2:19][CH2:20][NH2:21])[CH2:15][CH2:14]2)=[CH:5][CH:4]=1.[S:22]([Cl:32])([C:25]1[CH:31]=[CH:30][C:28]([CH3:29])=[CH:27][CH:26]=1)(=[O:24])=[O:23]>C(Cl)(Cl)Cl>[ClH:32].[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[N:13]2[CH2:18][CH2:17][N:16]([CH2:19][CH2:20][NH:21][S:22]([C:25]3[CH:31]=[CH:30][C:28]([CH3:29])=[CH:27][CH:26]=3)(=[O:24])=[O:23])[CH2:15][CH2:14]2)=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 73974-Toluenesulfonyl chlorideHCID 19808484HCID 19808484, compound

Product 1

HCID 19808482HCID 19808482, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

This compound was prepared according to the method described in Example 1, Stage E, from 1-(7-methoxy-1-naphthyl)-4-(2-aminoethyl)piperazine and tosyl chloride in solution in chloroform.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-c1b9eb1880f24f0494df1043bdbe9833
Source dataset
uspto-grants-1992_09
Patent number
US05143916

Reaction notes

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