HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 19808496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(7-Methoxynaphthalen-1-yl)piperazine | HCID 14566720 | — |
| Reactant | 2-Bromoethylphthalimide | HCID 21960021 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19808496 | HCID 19808496 | 63% |
Reaction Steps
A mixture of 1.5 g of (7-methoxy-1-naphthyl)piperazine and 1.5 g of (2-bromoethyl)phthalimide in 100 ml of acetone is brought to reflux in the presence of 1.6 g of potassium carbonate. The mixture is stirred for 24 hours. The mixture is cooled, it is concentrated. The oil obtained is ground in ether. The requisite quantity of ethereal hydrogen chloride is added to obtain the expected hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05143916 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-9870f1cd142e497db91c864b63298c7e |
| Source note | uspto-grants-1992_09 |