HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoroaniline → HCID 178450490, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoroaniline | HCID 9584 | — |
| Reactant | Ethyl 2-butyryl-3-ethoxyacrylate | HCID 3359484 | — |
| Product | HCID 178450490 | HCID 178450490 | 58.4% |
Reaction Steps
2-Fluoroaniline (25 g, 0.23 mol) and ethyl 2-butyryl-3-ethoxyacrylate (48 g, 0.23 mol) were heated at 150° for 2 hours, then diluted with petroleum ether and left to stand overnight. Filtration and washing gave ethyl 2-butyryl-3-(2-fluorophenylamino)acrylate (37.5 g), m.p. 60°-62°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05143920 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-cadb5ddf88fa47e49262cefeac66d979 |
| Source note | uspto-grants-1992_09 |