HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 19880164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Methoxybenzyl bromide | HCID 165021 | — |
| Reactant | 2-Chloro-3,4-dihydroxybenzoic acid | HCID 15608164 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19880164 | HCID 19880164 | — |
Reaction Steps
2-Chloro-3,4-dihydroxybenzoic acid is p-methoxybenzylated with potassium carbonate and p-methoxybenzyl bromide in dimethylformamide to give p-methoxybenzyl 2-chloro-3,4-bis(p-methoxybenzyloxy)benzoate. This is hydrolyzed with sodium hydroxide to give 2-chloro-3,4-bis(p-methoxybenzyloxy)benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05143910 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-169b281015cf4e8e8014796626546f75 |
| Source note | uspto-grants-1992_09 |