Aluminium lithium hydride → HCID 54335688, compound

HRID 1885296Notes

Reaction equation

HRID 1885296 reaction equation
[H-].[Al+3].[Li+].[H-].[H-].[H-].[S:7]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][S:20][C:21]1[CH:29]=[CH:28][CH:27]=[CH:26][C:22]=1[C:23](O)=[O:24])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>O1CCCC1>[S:7]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][S:20][C:21]1[CH:29]=[CH:28][CH:27]=[CH:26][C:22]=1[CH2:23][OH:24])[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1

Participants

4

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 85590543HCID 85590543, compound

Product 1

HCID 54335688HCID 54335688, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent2×

Procedure

To a suspension of lithium aluminum hydride (0.292 g, 0.007 mole) in tetrahydrofuran (30 ml) is added a solution of 2-(6-thiophenoxyhexylthio)benzoic acid (2.42 g, 0.007 mole) in tetrahydrofuran (30 ml). The reaction is conducted as in Example 1b).

Sources & evidence

ORD record
ord-49eebe7e775547e681ce4b68fdbf9e75
Source dataset
uspto-grants-1992_09
Patent number
US05143931

Reaction notes

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