反应详情

To a solution of 5.0 g of 2-[(hexadecyloxy)methyl]-2-propen-1-ol in 50 ml of dry N,N-dimethylformamide is added 6.05 g of tert-butyldimethylsilyl chloride followed by 8 g of imidazole. This mixture is stirred overnight, then diluted with ether, washed with saturated aqueous sodium bicarbonate, water and brine, dried and evaporated, to give 6.49 g of the desired compound.

1. washwashed with saturated aqueous sodium bicarbonate, water and brine
2. customdried
3. customevaporated