Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Butyl Chloride | HCID 8005 | — |
| Reactant | Magnesium | HCID 5462224 | — |
| Solvent | Methylcyclohexane | HCID 7962 | — |
| Product | HCID 178448198 | HCID 178448198 | — |
Reaction Steps
A volume of 23.7 ml (20.8 g, 0.225 moles) of n-butyl chloride was added gradually to a slurry of 6.8 g (0.25 g moles) of magnesium powder in 175 ml of methylcyclohexane at reflux (100° C.). After addition was complete, the mixture was refluxed for an additional 1-2 hours and allowed to cool to room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05145600 |
|---|
| Source dataset | uspto-grants-1992_09 |
|---|
| ORD ID | ord-ff010e6fc5c24c99900b995e19522947 |
|---|
| Source note | uspto-grants-1992_09 |
|---|
