Butyl Chloride → HCID 178448198, compound

HRID 1885503Notes

Reaction equation

HRID 1885503 reaction equation
[CH2:1]([Cl:5])[CH2:2][CH2:3][CH3:4].[Mg:6]>CC1CCCCC1>[Cl-:5].[Mg+2:6].[CH2:1]([Mg:6][CH2:1][CH2:2][CH2:3][CH3:4])[CH2:2][CH2:3][CH3:4].[Cl-:5]

Participants

4

Reactant 2

HCID 8005Butyl ChlorideHCID 5462224Magnesium

Product 1

HCID 178448198HCID 178448198, compound

Reagents, catalysts & solvents 1

HCID 7962MethylcyclohexaneSolvent

Conditions

Temperature
100 °C

Procedure

A volume of 23.7 ml (20.8 g, 0.225 moles) of n-butyl chloride was added gradually to a slurry of 6.8 g (0.25 g moles) of magnesium powder in 175 ml of methylcyclohexane at reflux (100° C.). After addition was complete, the mixture was refluxed for an additional 1-2 hours and allowed to cool to room temperature.

Workup

  1. additionAfter addition
  2. temperaturethe mixture was refluxed for an additional 1-2 hours
  3. temperatureto cool to room temperature

Sources & evidence

ORD record
ord-ff010e6fc5c24c99900b995e19522947
Source dataset
uspto-grants-1992_09
Patent number
US05145600

Reaction notes

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