HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 19878909, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Methyl adipate | HCID 6994472 | — |
| Product | HCID 19878909 | HCID 19878909 | — |
Reaction Steps
Chloro methyl adipate was prepared from mono-methyl adipate (10 g, 62.4 mmol) by refluxing with thionyl chloride (20 mL) for 2 h. Distillation gave the acid chloride (bp 80° C., 0.35 mm Hg, 7.4 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05145790 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-8cf25b3112cc4f46a2a7f0b806d2c945 |
| Source note | uspto-grants-1992_09 |