Dimethylamine, hydrochloride → HCID 19879202, compound

HRID 1885543Notes

Reaction equation

HRID 1885543 reaction equation
[CH2:1]([O:3][C:4]([CH2:6][C:7](=[NH:11])OCC)=[O:5])[CH3:2].[ClH:12].[CH3:13][NH:14][CH3:15]>C(O)C>[ClH:12].[CH3:13][N:14]([CH3:15])[C:7](=[NH:11])[CH2:6][C:4]([O:3][CH2:1][CH3:2])=[O:5]

Participants

4

Reactant 2

HCID 10473Dimethylamine, hydrochlorideHCID 75346Propanoic acid, 3-ethoxy-3-imino-, ethyl ester

Product 1

HCID 19879202HCID 19879202, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

107.3 g (0.67 mol) of the compound from Example 2 and 55 g (0.67 mol) of dimethylamine hydrochloride in 300 ml of ethanol are heated under reflux overnight. The solvent is removed by distillation and the residue is triturated with acetone

Workup

  1. temperatureunder reflux overnight
  2. customThe solvent is removed by distillation
  3. customthe residue is triturated with acetone

Sources & evidence

ORD record
ord-9e25857d34284720b7df57c93d5f8e56
Source dataset
uspto-grants-1992_09
Patent number
US05145857

Reaction notes

Loading…