HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → HCID 19025862, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 3-Iodo-1-phenylpropan-1-ol | HCID 14476874 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19025862 | HCID 19025862 | — |
Reaction Steps
(Compound 15) (12.5 g) was treated with butylamine (40 ml) in THF (75 ml) at RT for 4 h. The mixture evaporated and the residue extracted with OH- /ether. The ether phase washed with H2O and saturated NaCl-solution, dried (MgSO4) and evaporated giving 6.2 g of 3-butylamino-1-phenyl-1-propanol (compound 16). Identified by 1H NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05145870 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-7d8142389cfc49c581c24b858c4ab23d |
| Source note | uspto-grants-1992_09 |