m-Chloroperbenzoic acid → HCID 19879318, compound

Participants

Reaction Steps

0.75 g of m-chloroperbenzoic acid is added to a stirred solution of 0.6 g of 3-(5-chlorothiophen-2-yl)-prop-2-enol according to c) in 50 ml of dichloromethane. The solution is stirred at room temperature for 5 hours, washed with 10% sodium carbonate solution, dried over sodium sulfate and concentrated by evaporation. The residue is chromatographed on silica gel with ether and the title compound is obtained in the form of a light-yellow oil.

Provenance & Evidence