HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → 88708-72-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | Acetamide, N-[(4-chlorophenyl)methyl]-2,2,2-trifluoro- | HCID 580806 | — |
| Product | 88708-72-9 | HCID 10988866 | 61.5% |
Reaction Steps
A mixture N-(p-chlorobenzyl)-2,2,2-trifluoroacetamide (100.0 g, 0.421 mol) and phosphorus pentachloride (87.7 g, 0.421 mol) is heated to 100° C., stirred for two hours and vacuum distilled to obtain the title product as a clear colorless liquid (66.3 g, bp 110°-112° C./7.5 mm Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05145986 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-e2e4e739949640e5a857ed4741792eba |
| Source note | uspto-grants-1992_09 |