HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 15634838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 12139742 | HCID 12139742 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15634838 | HCID 15634838 | — |
Reaction Steps
A solution of methylamine in dry ethanol was added to a solution of (3S,4R)-6-cyano-3,4-dihydro-3,4-epoxy-2,2-dimethyl-2H-1-benzopyran* (1.0 g) in dry ethanol, and the resulting solution stirred at room temperature for 2 days. Evaporation of solvent in vacuo gave the title compound as a gum (1.0 g) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05147866 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-6bbc2a9263114a0f8b3dc3cd3c0a18e0 |
| Source note | uspto-grants-1992_09 |