HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Benzoxazolinone, 3-methyl- → 3-Methyl-6-(pyridine-3-carbonyl)-1,3-benzoxazol-2(3H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Benzoxazolinone, 3-methyl- | HCID 30846 | — |
| Reactant | 3-Pyridinecarbonyl chloride, hydrochloride (1:1) | HCID 88438 | — |
| Product | 3-Methyl-6-(pyridine-3-carbonyl)-1,3-benzoxazol-2(3H)-one | HCID 15171439 | — |
Reaction Steps
The flask is equipped with a reflux condenser and taken to an oil bath at a temperature in the region of 45° C. 6 g (0.04 mol) of 3-methylbenzoxazolinone and 10.6 g (0.06 mol) of nicotinoyl chloride hydrochloride are introduced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05147883 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-7240b55f14fc490aa589981bb11f01fd |
| Source note | uspto-grants-1992_09 |