HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 15129665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Piperidine, 1-(2-chloroethyl)-, hydrochloride | HCID 74826 | — |
| Reactant | HCID 15129664 | HCID 15129664 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15129665 | HCID 15129665 | — |
Reaction Steps
A 1.8 g portion of the compound of Example 3 was combined with 3.4 g of potassium carbonate, 0.95 g of 1-(2-chloroethyl)piperidine hydrochloride and 20 ml of dimethylformamide, and the reaction was carried out and the product was isolated as described above in Example 6. The chromatography gave 2.05 g of purified product, which was recrystallized from ethyl acetate/isooctane to obtain 1.93 g of highly purified product, m.p. 162°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05147880 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-c2bbd118ce974390940e152d0d8dc66f |
| Source note | uspto-grants-1992_09 |