HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 57324802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 22840453 | HCID 22840453 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 57324802 | HCID 57324802 | — |
Reaction Steps
The title compound is prepared analogously to Example 5a) from (2S,3S)-2,3-epoxy-3-(3-trifluoromethylphenyl)-propanol. Light-yellow liquid; IR (CH2Cl2): 2820, 1730, 1330, 1165, 1130, 1070 cm-1 ; [α]D20 (chloroform, 0.20%)=0.0°±5°; [α]36520 (chloroform, 0.20%)=475.0°±5.0°; Rf =0.44 (hexane/ethyl acetate 7:3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05149717 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-6f0ce3a084b54305acd3761c1d3fc276 |
| Source note | uspto-grants-1992_09 |