Hydrogen Peroxide → HCID 15746742, compound

Participants

Reaction Conditions

Reaction Steps

80 g (0.5 mol) of N-carbamoylsuccinamic acid are dissolved in 160 g of methanesulfonic acid and the solution is cooled to 15° C. 60 g (1.5 mol) of hydrogen peroxide (85% strength by weight) are added dropwise with cooling at such a rate that the internal temperature can be maintained between 15° and 20° C. The reaction mixture is stirred at 20° C. for 10 minutes, then cooled to 10° C. and admixed with water added dropwise with cooling. The precipitated peroxycarboxylic acid is filtered off with suction, washed free of mineral acid with water and dried at 40° C. under an aspirator vacuum.

Provenance & Evidence