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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1886317Generated: November 2, 2026

2',4'-Dihydroxyacetophenone → HCID 135708777, compound

https://huagongshe.com/reaction/1886317

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2',4'-DihydroxyacetophenoneHCID 6990—
Reactant6-(4-Aminophenyl)-4,5-dihydropyridazin-3(2H)-oneHCID 676750—
ProductHCID 135708777HCID 135708777—

Reaction Conditions

Temperature140 °C

Reaction Steps

A mixture containing 0.91 g (0.006 mol) of 2',4'-dihydroxyacetophenone and 0.95 g (0.005 mol) of 6-(4-aminophenyl)-4,5-dihydropyridazin-3(2H)one was heated for 4 h at 140° C. in a stream of nitrogen gas. The product was triturated with boiling ethanol and filtered. Yield 0.88 g (54%), m.p. 350° C. (decomp).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05151420
Source datasetuspto-grants-1992_09
ORD IDord-61c1948d6623469aa5288dec273879e6
Source noteuspto-grants-1992_09