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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1886318Generated: November 4, 2026

2',4'-Dihydroxypropiophenone → HCID 136113993, compound

https://huagongshe.com/reaction/1886318

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2',4'-DihydroxypropiophenoneHCID 79856—
ReactantIci 109,081HCID 161928—
ProductHCID 136113993HCID 136113993—

Reaction Conditions

Temperature140 °C

Reaction Steps

A mixture of 0.167 g (0.0011 mol) of 2',4'-dihydroxypropiophenone and 0.203 g (0,001 mol) of 6-(4-aminophenyl)-4,5-dihydro-5-methylpyridazin-3(2H)one was heated for 1 h at 140° C. The product was triturated with ethanol and filtered. Yield 0.15 g (45%), m.p. 185°-190° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05151420
Source datasetuspto-grants-1992_09
ORD IDord-d828bd7c8d854f1298c0e6a8a609d23c
Source noteuspto-grants-1992_09