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HRID1886319

反应详情

EQUATION

反应方程式

HRID 1886319 的结构方程式

REACTANTS

反应物

2
结构：CCC(=O)c1ccc(O)cc1O
HCID79856

2',4'-Dihydroxypropiophenone

C9H10O3

结构：Nc1ccc(C2=NNC(=O)CC2)cc1
HCID676750

6-(4-Aminophenyl)-4,5-dihydropyridazin-3(2H)-one

C10H11N3O

PRODUCTS

生成物

1
结构：CCC(=Nc1ccc(C2=NNC(=O)CC2)cc1)c1ccc(O)cc1O
HCID136160758

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)N(C)C
溶剂HCID31374

Dimethylacetamide

C4H9NO

CONDITIONS

反应条件

温度
140 °C

PROCEDURE

实验过程

A solution containing 1.0 g (0.006 mol) of 2',4'-dihydroxypropiophenone and 0.57 g (0.003 mol) of 6-(4-aminophenyl)-4,5-dihydropyridazin-3(2H)one in 10 ml of DMA was heated for 20 h at 140° C. The solvent was evaporated in vacuo and the residue was crystallized from ethanol. Yield 0.05 g (5%), m.p. 350° C. (decomp).

WORKUP

后处理

  1. customThe solvent was evaporated in vacuo
  2. customthe residue was crystallized from ethanol