HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 14601681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Reactant | 4-(Trifluoromethyl)benzaldehyde | HCID 67996 | — |
| Reactant | HCID 20326490 | HCID 20326490 | — |
| Product | HCID 14601681 | HCID 14601681 | — |
Reaction Steps
A solution containing 0.87 g of 4-trifluoromethylbenzaldehyde, 6-(4-aminophenyl-4,5-dihydropyridazin-3(2H)one, 1 ml of acetic acid and 10 ml of N,N-dimethylacetamide in 40 ml of ethanol was refluxed for 5 h. The product was filtered and washed with ethanol. Yield 0.7 g (41%), m.p. 245°-247° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05151420 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-fbc38182c0df4a9d978321fa73d383c0 |
| Source note | uspto-grants-1992_09 |