HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → HCID 19875819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 6-(3,4-Diaminophenyl)-5-methyl-4,5-dihydropyridazin-3(2H)-one | HCID 3441052 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19875819 | HCID 19875819 | — |
Reaction Steps
A solution containing 0.3 g of 6-(3,4-diaminophenyl)-5-methyl-4,5-dihydropyridazin-3(2H)one, 0.3 g of phenacyl bromide and 0.14 g of sodium acetate in 2.6 ml of ethanol was stirred for 3.5 h at room temperature. The product was washed with water and ethanol. Yield 0.1 g (23%), m.p. 209°-215° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05151420 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-701059384d6047d08d962f2814405ea2 |
| Source note | uspto-grants-1992_09 |