Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 70044523 | HCID 70044523 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 11557656 | HCID 11557656 | — |
Reaction Steps
L-Leucyl-L-prolinamide hydrobromide (517 mg) was dissolved in DMF (1.5 ml), to which was added triethylamine (0.35 ml) under cooling at -10° C. The mixture was stirred for 10 minutes under ice-cooling and the resultant precipitate was filtered off to give L-leucyl-L-prolinamide in DMF solution, which was immediately used for the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05151497 |
|---|
| Source dataset | uspto-grants-1992_09 |
|---|
| ORD ID | ord-c7f6d573d3294e99a72d387976fe8093 |
|---|
| Source note | uspto-grants-1992_09 |
|---|
