Sodium Hydroxide → HCID 14534580, compound

HRID 1886557Notes

Reaction equation

HRID 1886557 reaction equation
C([O:4][CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]([CH3:14])[CH3:13])[C:7]=1[Br:15])(=O)C.[OH-].[Na+]>O1CCOCC1>[Br:15][C:7]1[C:8]([CH:12]([CH3:14])[CH3:13])=[CH:9][CH:10]=[CH:11][C:6]=1[CH2:5][OH:4]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 14534579HCID 14534579, compound

Product 1

HCID 14534580HCID 14534580, compoundYield 99.7%

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

116 g (0.43 mole) of 2-bromo-3-isopropylbenzyl acetate in 770 ml of dioxane and 255 g of 8% strength sodium hydroxide solution are hydrolyzed and worked up similarly to Example 1, Paragraph c. 98.2 g (quantitative) of 2-bromo-3-isopropylbenzyl alcohol of boiling point 110°-112° C./0.2 mbar are obtained.

Sources & evidence

ORD record
ord-4a775d23a1d6420bbc90e6287d01f6ab
Source dataset
uspto-grants-1992_09
Patent number
US05151548

Reaction notes

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