HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 14534580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14534579 | HCID 14534579 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 14534580 | HCID 14534580 | 99.7% |
Reaction Steps
116 g (0.43 mole) of 2-bromo-3-isopropylbenzyl acetate in 770 ml of dioxane and 255 g of 8% strength sodium hydroxide solution are hydrolyzed and worked up similarly to Example 1, Paragraph c. 98.2 g (quantitative) of 2-bromo-3-isopropylbenzyl alcohol of boiling point 110°-112° C./0.2 mbar are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05151548 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-4a775d23a1d6420bbc90e6287d01f6ab |
| Source note | uspto-grants-1992_09 |