HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → 2-(12-Phthalimido dodecyl)propane dioic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 2-(12-Phthalimido dodecyl)propane dioic acid di-tert-butyl ester | HCID 86648912 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-(12-Phthalimido dodecyl)propane dioic acid | HCID 86648911 | 100% |
Reaction Steps
Following general procedure D, 16.0 mmol (8.45 g) of 5c and 160 mmol (11.9 mL) of trifluoroacetic acid were reacted in 12 mL of dichloromethane at room temperature and the mixture was processed. Yield 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501199B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-2c5e79c602a84d9fa0caec80d5c30337 |
| Source note | uspto-grants-2013_08 |