HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 131730750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Fmoc-O-benzyl-L-serine | HCID 7017914 | — |
| Reactant | 2-(2,5-Dioxopyrrolidin-1-yl)-1,1,3,3-tetramethylisouronium tetrafluoroborate | HCID 9857522 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131730750 | HCID 131730750 | — |
Reaction Steps
FmocSer(Bzl) (1 mmol), TSTU (1 mmol), and DIEA (2 mmol) were dissolved in DMF (6 mL). The mixture was shaken at room temperature for half an hour. The solvent was evaporated to form FmocSer(Bzl)-OSu, which was used directly in the following steps.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501498B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-a55f0450ffed471897ded4bcad490ec8 |
| Source note | uspto-grants-2013_08 |