HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminophenylboronic acid → HCID 58006551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminophenylboronic acid | HCID 2734615 | — |
| Reactant | 4-(Tetramethyl-1,3,2-dioxaborolan-2-yl)aniline | HCID 2734620 | — |
| Reactant | 1-(6-Chloro-pyridazin-3-yl)-4-isopropyl-perhydro-1,4-diazepine | HCID 86637103 | — |
| Product | HCID 58006551 | HCID 58006551 | — |
Reaction Steps
The title compound was prepared by a similar procedure to that described in Example 68, starting from 1-(6-chloro-pyridazin-3-yl)-4-isopropyl-perhydro-1,4-diazepine and 4-aminophenylboronic acid, pinacol cyclic ester. 1H NMR (400 MHz, CDCl3) δ 7.82 (d, 2H), 7.53 (d, 1H), 6.76 (m, 3H), 3.86 (t, 2H), 3.77 (m, 4H), 2.93 (heptet, 1H), 2.81 (m, 2H), 2.58 (m, 2H), 1.95 (m, 2H), 1.00 (d, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501739B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-9ee0771ec86a4e838f4e23c8ae58e9d6 |
| Source note | uspto-grants-2013_08 |