HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4'-Bipiperidine → 1'-[6-(Pyridin-3-yl)pyridazin-3-yl]-1,4'-bipiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4'-Bipiperidine | HCID 78607 | — |
| Reactant | 3-Chloro-6-(pyridin-3-yl)pyridazine | HCID 16732435 | — |
| Product | 1'-[6-(Pyridin-3-yl)pyridazin-3-yl]-1,4'-bipiperidine | HCID 58006568 | — |
Reaction Steps
The title compound was prepared by a similar procedure to that described in Example 1, starting from 3-chloro-6-(pyridin-3-yl)-pyridazine and 4-piperidinopiperidine. 1H NMR (400 MHz, CD3OD) δ 9.47 (d, 1H), 9.11 (dt, 1H), 8.93 (d, 1H), 8.40 (d, 1H), 8.15 (q, 1H), 7.94 (d, 1H), 4.66 (d, 2H), 3.66 (m, 1H), 3.58 (d, 2H), 3.36 (t, 2H), 3.08 (t, 2H), 2.38 (d, 2H), 1.80-2.00 (m, 7H), 1.54 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501739B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-fcfb01bf151144a287d88b1aa1aa0ad1 |
| Source note | uspto-grants-2013_08 |