Diiodomethane → HCID 54390712, compound

HRID 1887204Notes

Reaction equation

HRID 1887204 reaction equation
N[C:2]1[C:3]([CH3:9])=[N:4][CH:5]=[CH:6][C:7]=1[CH3:8].N(OCCC(C)C)=O.C(I)[I:19]>>[I:19][C:2]1[C:3]([CH3:9])=[N:4][CH:5]=[CH:6][C:7]=1[CH3:8]

Participants

4

Reactant 3

HCID 6346DiiodomethaneHCID 8053Isoamyl NitriteHCID 149107812,4-Dimethylpyridin-3-amine

Product 1

HCID 54390712HCID 54390712, compound

Procedure

In a manner similar to that described in Example 5 (Step 1), commercially available 3-amino-2,4-dimethylpyridine was treated with isoamyl nitrite and CH2I2 to provide 3-iodo-2,4-dimethylpyridine (16A).

Sources & evidence

ORD record
ord-90ef4b7a87104063bdb08fc430707ed2
Source dataset
uspto-grants-2013_08
Patent number
US08501747B2

Reaction notes

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