HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N,N',N'-Tetramethylethylenediamine → HCID 59483440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N,N',N'-Tetramethylethylenediamine | HCID 8037 | — |
| Reactant | N-Methylbutylamine | HCID 8068 | — |
| Reactant | HCID 25159695 | HCID 25159695 | — |
| Reactant | HCID 178418416 | HCID 178418416 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 59483440 | HCID 59483440 | — |
Reaction Steps
The following are reacted at 30 bar and 130° in an autoclave: 100 mg of 2-amino-6-bromo-4-diethylcarbamoylquinazoline, 30 ml of 1,4-dioxane, 7 ml of carbon monoxide, 10 mg of (1,1′-bis(diphenylphosphino)-ferrocene)dichloropalladium(II), 50 mg of N,N,N′,N′-tetramethylethylene-diamine and 80 mg of N-methylbutylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501754B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-8ecb65c2a0d849afa020a2b823d19b78 |
| Source note | uspto-grants-2013_08 |