TFA dichloromethane water → HCID 86761991, compound

Participants

Reaction Steps

A solution of 2-[4-(2,2-dimethoxyethoxy)-3-methoxyphenyl]-6-[(S)-1-(tetrahydrofuran-2-yl)methoxy]-2H-isoquinolin-1-one (94 mg) in 10:10:1 TFA/dichloromethane/water (2 mL) was stirred at room temperature for 2 h. The solvent was removed in vacuo. The product with the molecular weight of 409.44 (C23H23NO6) was obtained in this way; MS (ESI): 428 (M+water+H+).

Provenance & Evidence