HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aspirin → HCID 86648420, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aspirin | HCID 2244 | — |
| Reactant | Donepezil | HCID 3152 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86648420 | HCID 86648420 | — |
Reaction Steps
3.79 g of Donepezil is dissolved in 70 ml of ethyl acetate, and a solution of acetylsalicylic acid (1.80 g) in acetone (35 ml) is added slowly with stirring at room temperature. The solid precipitated is filtered. Melting point: 173-176° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501779B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-5d80dd6e7df542c782ebd38dcc1483a3 |
| Source note | uspto-grants-2013_08 |