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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1888222생성일: 2026년 10월 25일

HCID 178477695, 화합물 → HCID 178477694, 화합물

https://huagongshe.com/reaction/1888222

반응식

참여 물질

역할이름HCID투입량
반응물HCID 178477695HCID 178477695—
촉매Manganese dioxideHCID 14801—
용매TetrahydrofuranHCID 8028—
생성물HCID 178477694HCID 178477694—

반응 단계

To a solution of 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-[3-(hydroxymethyl)phenyl]-1H-indazole-7-carboxamide (Intermediate 23) (130 mg, 0.294 mmol) in THF (50 mL) was added MnO2 (900 mg, 8.8 mmol). The reaction mixture was stirred at room temperature overnight and filtered. The filtrate was concentrated at reduced pressure to give the crude title compound, which was used in the next step without further purification.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08501780B2
출처 데이터셋uspto-grants-2013_08
ORD IDord-bf1020875a604530a53e9e5b08318098
출처 메모uspto-grants-2013_08