HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethylhexyl 3-mercaptopropionate → 2-Ethylhexyl 3-{[5-(benzyloxy)-2-nitrophenyl]sulfanyl}propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethylhexyl 3-mercaptopropionate | HCID 92640 | — |
| Reactant | 4-Benzyloxy-2-fluoro-1-nitrobenzene | HCID 22180704 | — |
| Product | 2-Ethylhexyl 3-{[5-(benzyloxy)-2-nitrophenyl]sulfanyl}propanoate | HCID 58047380 | 100.3% |
Reaction Steps
Using 4-(benzyloxy)-2-fluoro-1-nitrobenzene (10.3 g, 41.6 mmol) and 2-ethylhexyl 3-sulfanylpropanoate (10.0 g, 45.8 mmol) and in the same manner as in Reference Example 81, the title compound (18.6 g, quantitative) was obtained as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501804B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-46b8181a774b4598b66b3d025758d817 |
| Source note | uspto-grants-2013_08 |