HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-N-Boc-aminopropionic acid → HCID 70228130, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-N-Boc-aminopropionic acid | HCID 268471 | — |
| Reactant | 2-Amino-4-methoxyphenol | HCID 1419108 | — |
| Product | HCID 70228130 | HCID 70228130 | 81% |
Reaction Steps
Using 2-amino-4-methoxyphenol (3.00 g, 21.6 mmol) and N-(tert-butoxycarbonyl)-D,L-alanine (4.08 g, 21.6 mmol), a method in the same manner as in Reference Example 13 was performed, and the obtained residue was triturated with ethyl acetate to give the title compound (5.42 g, yield 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501804B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-53392665b3f441b29d2647e4094af439 |
| Source note | uspto-grants-2013_08 |