HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 58047521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromoacetone | HCID 11715 | — |
| Reactant | HCID 57425030 | HCID 57425030 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 58047521 | HCID 58047521 | 72.4% |
Reaction Steps
Using 5-chloro-2-hydroxy-4-(methoxymethoxy)benzaldehyde (1.50 g, 6.94 mmol), acetonitrile (14 mL), bromoacetone (1.57 g, 10.4 mmol) and potassium carbonate (2.87 g, 20.8 mmol), an operation in the same manner as in Reference Example 86 was performed to give the title compound (1.28 g, yield 72%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501804B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-7859d80167c849ba9e0111bb279cf8dc |
| Source note | uspto-grants-2013_08 |