HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2R)-oxolan-2-ylmethanol → HCID 58047354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2R)-oxolan-2-ylmethanol | HCID 6931745 | — |
| Reactant | Methyl 2-fluoro-4-hydroxybenzoate | HCID 22463192 | — |
| Product | HCID 58047354 | HCID 58047354 | 98% |
Reaction Steps
Using (2R)-tetrahydrofuran-2-ylmethanol (1.71 g, 10.0 mmol) and methyl 2-fluoro-4-hydroxybenzoate (1.24 g, 12.0 mmol) obtained in Reference Example 272 and in the same manner as in Reference Example 273, the title compound (2.49 g, yield 98%) was obtained as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501804B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-51e50d5372654f2ca78ca78065d58864 |
| Source note | uspto-grants-2013_08 |