HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl methyl sulfide → HCID 58047280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl methyl sulfide | HCID 10965 | — |
| Reactant | HCID 58047041 | HCID 58047041 | — |
| Product | HCID 58047280 | HCID 58047280 | 50% |
Reaction Steps
Using N-(1-{6-[2-(4-hydroxyphenyl)ethyl]-1-benzofuran-2-yl}ethyl)acetamide (150 mg, 0.464 mmol) obtained in Example 165 and 2-chloroethylmethylsulfide (0.182 mL, 1.86 mmol) and in the same manner as in Example 158, the title compound was obtained (91.9 mg, yield 50%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501804B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-304c560b98114bcf87ee5c7bc9c847ea |
| Source note | uspto-grants-2013_08 |