HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 3-(2,2-Dimethylpropyl)-5,6,7,8-tetrahydro-5,8-ethanocinnoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Bicyclo[2.2.2]octane-2,3-dione | HCID 548936 | — |
| Reactant | (4,4-Dimethyl-2-oxo-pentyl)-phosphonic acid dimethyl ester | HCID 25112585 | — |
| Product | 3-(2,2-Dimethylpropyl)-5,6,7,8-tetrahydro-5,8-ethanocinnoline | HCID 46175328 | — |
Reaction Steps
White solid MS (ESI): 231.1 (MH+). Prepared from bicyclo[2.2.2]octane-2,3-dione, (4,4-dimethyl-2-oxo-pentyl)-phosphonic acid dimethyl ester, hydrazine monohydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501940B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-ed171f453f6b406da2ed572e56693259 |
| Source note | uspto-grants-2013_08 |